Parr-instrument Series 4558 User Manual

403M4555-45585G & 10L Pressure ReactorsOperating Instruction Manual

4555 - 58 Series 5G & 10L Pressure Reactors - 9 - ASSEMBLE THE REACTOR These reactors require a work area in a well ventilated area with c

4555 - 58 Series 5G & 10L Pressure Reactors - 10 - Fixed Head Vessel Caution Symbols: 1. For the apparatus to be fully stable in a

4555 - 58 Series 5G & 10L Pressure Reactors - 11 - 8. Remove the front drive guard shield if applicable. Refer to drawing 4557 Sheet 2 in

4555 - 58 Series 5G & 10L Pressure Reactors - 12 - Slotted holes for center adjustment (Left/Right) (4) 5/16 x 1/2” Oversized holes for lev

4555 - 58 Series 5G & 10L Pressure Reactors - 13 - IDENTIFY THE VALVES Gas Inlet Valve The gas inlet valve is easily identified when the v

4555 - 58 Series 5G & 10L Pressure Reactors - 14 - OTHER VESSEL HEAD FITTINGS Safety Rupture Disc There is a safety rupture disc attached

4555 - 58 Series 5G & 10L Pressure Reactors - 15 - HOW TO USE THE VESSEL The vessels used in Model 4555, 4556, 4557, 4558, 4667 and 4668 Re

4555 - 58 Series 5G & 10L Pressure Reactors - 16 - Close the Vessel For removable heads, lift the head carefully from its service position

4555 - 58 Series 5G & 10L Pressure Reactors - 17 - flow control valve on the gas tank closed, open the main valve on the gas tank only abou

4555 - 58 Series 5G & 10L Pressure Reactors - 18 - REACTORS WITH SLAVE BOX CONTROLS Reactors can be set up with a wide variety of heaters.

4555 - 58 Series 5G & 10L Pressure Reactors - 19 - ACCESSORIES Internal Cooling Coils Cooling coils can be installed in any of these react

4555 - 58 Series 5G & 10L Pressure Reactors - 20 - Air Motor Variable stirring speeds from 100 to 2000 rpm can be obtained by replacing the

4555 - 58 Series 5G & 10L Pressure Reactors - 21 - EXPLOSION PROOF OPERATION If the local safety code requires that equipment installed in

4555 - 58 Series 5G & 10L Pressure Reactors - 22 - PERIODIC PRESSURE TESTS Each cylinder used in a Parr stirred reactor is tested under hy

4555 - 58 Series 5G & 10L Pressure Reactors - 23 - GENERAL MAINTENANCE NOTES 1. Periodically inspect all electrical wiring and pressure co

4555 - 58 Series 5G & 10L Pressure Reactors - 24 - 10. To operate reactors equipped with an air motor, connect air hose to a compressed ai

4555 - 58 Series 5G & 10L Pressure Reactors - 25 - PARTS LISTS Vessel Parts List Consult the itemized list of part numbers provided with

4555 - 58 Series 5G & 10L Pressure Reactors - 26 - Internal Fittings continued Shafts 1025HC28 Upper Stub Shaft 5G Magnetic Drive A1030HC

4555 - 58 Series 5G & 10L Pressure Reactors - 27 - Internal Parts Identification 4555 / 4557 5 Gallo

4555 - 58 Series 5G & 10L Pressure Reactors - 28 - External Parts Identification

4555 - 58 Series 5G & 10L Pressure Reactors - 2 - TABLE OF CONTENTS TABLE OF CONTENTS... 2 Related Instructions...

4555 - 58 Series 5G & 10L Pressure Reactors - 29 - Cooling Coils & Fittings 1568HC Serpentine Cooling Coil, 3/8T, 5G 2968HC Serpen

4555 - 58 Series 5G & 10L Pressure Reactors - 30 - Drive Parts List Motor A388E2ES Motor, 1/2 HP VS 90VDC A388E2EQ Motor, 1/2 HP EXP V

4555 - 58 Series 5G & 10L Pressure Reactors - 31 - Stands Stand Parts (Fixed Head Vessel) A2760HC2 Pneumatic Lift Package with Regulator

4555 - 58 Series 5G & 10L Pressure Reactors - 32 - Heaters A1590HCEE 3-Zone Ceramic Heater Assembly (Removable Vessel) 83E Locknut 460E

4555 - 58 Series 5G & 10L Pressure Reactors - 33 - APPENDIX A – REMOVABLE VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 34 - APPENDIX A – REMOVABLE VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 35 - APPENDIX A – REMOVABLE VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 36 - APPENDIX B – 5-GALLON, FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 37 - APPENDIX B – 10-LITER FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 38 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 3 - _________________________________ Related Instructions The following Parr publications are a

4555 - 58 Series 5G & 10L Pressure Reactors - 39 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 40 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 41 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 42 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 43 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 44 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 45 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

4555 - 58 Series 5G & 10L Pressure Reactors - 46 - APPENDIX B – FIXED HEAD VESSEL REACTOR DRAWINGS

Revision 11/16/12

4555 - 58 Series 5G & 10L Pressure Reactors - 4 - PREFACE Scope These instructions include information for the installation and operation of st

4555 - 58 Series 5G & 10L Pressure Reactors - 5 - General Specifications Electrical Ratings Controller ratings are found in the Operating Instru

4555 - 58 Series 5G & 10L Pressure Reactors - 6 - Explanation of Symbols I On position O Off position ~ Alternating current (AC) 3 ~ Three–phase

4555 - 58 Series 5G & 10L Pressure Reactors - 7 - Intended Usage This system has been designed for use as a high pressure reactor system. I

4555 - 58 Series 5G & 10L Pressure Reactors - 8 - INSTALLATION Pressure and Temperature Limits The working pressure and temperature at whi