Parr-instrument Series 5500 User Manual

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Summary of Contents

Page 1 - Operating Instruction Manual

443M5500Compact Mini Bench Top ReactorsOperating Instruction Manual

Page 2 - Parr Instrument Company

Compact Mini Bench Top ReactorsParr Instrument Company10IDENTIFY THE VALVES Gas Inlet ValveThe gas inlet valve is easily identified when the vessel is

Page 3

Compact Mini Bench Top Reactorswww.parrinst.com11OTHER VESSEL HEAD FITTINGS Safety Rupture DiscThere is a safety rupture disc attached to the head whi

Page 4 - Cleaning & Maintenance

Compact Mini Bench Top ReactorsParr Instrument Company12HOW TO USE THE VESSELTo open the Vessel Open the gas release valve to discharge any internal

Page 5 - User’s Responsibility

Compact Mini Bench Top Reactorswww.parrinst.com13With the inlet valve open and the flow control valve on the gas tank closed, open the main valve on th

Page 6 - INSTALLATION

Compact Mini Bench Top ReactorsParr Instrument Company14MAINTENANCEGeneral Maintenance Notes1. Periodically inspect all electrical wiring and pres-su

Page 7

Compact Mini Bench Top Reactorswww.parrinst.com15Technical SupportParr Instrument Company strives to provide our customers with world class support.

Page 8 - Assemble The Reactor

Compact Mini Bench Top ReactorsParr Instrument Company16PARTS LISTSVessel Closure and Standard Internal PartsVessel Closure and Standard External Part

Page 9

Compact Mini Bench Top Reactorswww.parrinst.com17Reaction Vessel Parts ListConsult the itemized list for your reactor provided along with this manual.

Page 10 - IDENTIFY THE VALVES

Compact Mini Bench Top ReactorsParr Instrument Company18External FittingsPart No. Description79HW* Plug, 1/8” NPTMA122VB Valve, straight 1/8” NPTMA146

Page 11 - ACCESSORIES

Compact Mini Bench Top Reactorswww.parrinst.com19Impellers*Part No. DescriptionA837HC Impeller with screwGaskets & SealsPart No. Description Code4

Page 12 - HOW TO USE THE VESSEL

Compact Mini Bench Top ReactorsParr Instrument Company2PREFACE 3Scope 3Related Instructions 3Intended Usage 3Safety Information 3General Spe

Page 13 - Initial Operating Test

Compact Mini Bench Top ReactorsParr Instrument Company20DRAWINGSMotor/Overarm LayoutTach Option Layout

Page 14 - MAINTENANCE

Compact Mini Bench Top Reactorswww.parrinst.com21100, 160, 300 mL Mini Compact Reactor 22.13 8.07 300mL MINI HEATER W/COOLINGA3061HC4EEGEN5500TACH (R

Page 15 - MOLINE, IL. USA

Compact Mini Bench Top ReactorsParr Instrument Company22450 mL Mini Compact Reactor 8.07 23.77 2.25 6.06450mL450mL19.21.06 GAPREF 9.28 A3061HC5EE450

Page 16 - PARTS LISTS

Compact Mini Bench Top Reactorswww.parrinst.com23600 mL Mini Compact Reactor 25.77 8.07 GEN5500MTR (REF PAGE 20)MOTOR/OVERARM PKGREF600mL VESSEL ASSY

Page 18 - Mini Head External Fittings

Compact Mini Bench Top Reactorswww.parrinst.com3PREFACEScopeThese instructions describe the installation, opera-tion and maintenance of Parr Series 55

Page 19 - Vessel Heaters Parts List

Compact Mini Bench Top ReactorsParr Instrument Company4Explanation of SymbolsII On position, full power heater switchI On position, half power heater

Page 20 - DRAWINGS

Compact Mini Bench Top Reactorswww.parrinst.com5User’s ResponsibilityAll Parr Reactors and Pressure Vessels are designed and manufactured with great c

Page 21

Compact Mini Bench Top ReactorsParr Instrument Company6INSTALLATIONFlat PTFE Gasket The flat gasket is held in a recess in the vessel head and a machin

Page 22 - 450 mL Mini Compact Reactor

Compact Mini Bench Top Reactorswww.parrinst.com7Pressure and Temperature LimitsWorking pressures up to 3000 psig (200 bar) maximum are permissible in

Page 23 - 600 mL Mini Compact Reactor

Compact Mini Bench Top ReactorsParr Instrument Company8Assemble The ReactorThese reactors require at least 3 sq. ft. of work space on a sturdy bench

Page 24 - 443M R07 12/11/14

Noteswww.parrinst.com9

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