Parr-instrument 6400 User Manual

Operating Instruction Manual 6400 Calorimeter 534M

6400 Calorimeter Instruction Manual 2-4 Fill the external rinse tank with about 16 liters of distilled water through the large opening at the top of

6400 Calorimeter Instruction Manual 14-1 TABLES Table 2 - Default Settings Calorimeter Operation Operating Mode Determination Bomb Installed/EE

6400 Calorimeter Instruction Manual 14-2 Table 3 - Default Settings Data Entry Controls Prompt for Bomb ID ON Weight Entry Mode Touch Screen Aci

6400 Calorimeter Instruction Manual 14-3 Table 4 - ISO & BSI Method Settings Page Line Setting Value Thermochemical Corrections Fixed Acid S

Printed 03/07/08 PARR INSTRUMENT COMPANY 211 Fifty - Third Street Moline, Illinois 61265 USA 309 / 762-7716 800 / 8

6400 Calorimeter Instruction Manual 2-5 Note: A hissing sound will occur while the rinse tank is being pressurized. This is normal. Adjust the pn

6400 Calorimeter Instruction Manual 2-6 Table 1 - 6400 Calorimeter Serial Ports Pin-Out 9 pin D Connector Pin # Description Direction (6400 – Ext

6400 Calorimeter Instruction Manual 2-7 Multiple Alternate Configurations Printer Connections The printer port settings are on the Communication C

6400 Calorimeter Instruction Manual 2-8 Mettler 011/012 Interface The ID field must contain “S_” to indicate a stable mass. The data field contain

6400 Calorimeter Instruction Manual 2-9 Computer Connections If the 6400 Calorimeter is to be connected to a computer, the Ethernet connection shoul

6400 Calorimeter Instruction Manual 2-10 The following screenshot illustrates the contents of the calorimeter data directory as presented by a web b

6400 Calorimeter Instruction Manual 2-11 The calorimeter offers a web server service. Test reports can be viewed with a web browser using a URL of

6400 Calorimeter Instruction Manual 2-12 Clicking on any given report will provide a display similar to the following:

6400 Calorimeter Instruction Manual 3-1 QUICK START 1. Turn on the heater and pump in the Calorimeter Operation menu. Allow at least 20 minutes f

6400 Calorimeter Instruction Manual TABLE OF CONTENTS TABLE OF CONTENTS ...

6400 Calorimeter Instruction Manual 4-1 OPERATION Menu System All configurations and operations are handled by a menu-driven system operated from t

6400 Calorimeter Instruction Manual 4-2 Control Keys There are five control keys which always appear in the right column of the primary displays. T

6400 Calorimeter Instruction Manual 4-3 To re-load the user default setting, go to the Program Info and Control Page, User/Factory Settings, Re-loa

6400 Calorimeter Instruction Manual 4-4 Sample Types Because of the difference in combustion characteristics of the many different materials which m

6400 Calorimeter Instruction Manual 4-5 who intend to test these materials are urged to select the 1138CL Bomb. These bombs are 250 mL in volume an

6400 Calorimeter Instruction Manual 4-6 4. Set the cup in the capsule holder and arrange the auxiliary fuse so that it touches the center of the ta

6400 Calorimeter Instruction Manual 4-7 When superior corrosion resistance is needed, the Platinum Rhodium 43A5 Capsule is required. Test Process L

6400 Calorimeter Instruction Manual 4-8 Notice that the bomb head grounding lug extends beyond the outside diameter of the bomb head. A slot for t

6400 Calorimeter Instruction Manual 4-9 2. The water fill solenoid opens and water is pumped from the internal tank into and through the bucket tha

6400 Calorimeter Instruction Manual 4-10 continues to circulate from the closed water system through the jacket surrounding the bucket. 2. The oxyg

6400 Calorimeter Instruction Manual Operating Controls Menu...

6400 Calorimeter Instruction Manual 4-11 Cool / Rinse At the completion of the post-period, the rinse and cool sequence begins. Figure 8 - Rinse &a

6400 Calorimeter Instruction Manual 4-12 Note: Several rinse patterns may be configured by the user to meet various operational and analytical requ

6400 Calorimeter Instruction Manual 4-13 Figure 9 - Drain Flow Diagram The water in the bucket is drained out of the bucket and routed to the drain

6400 Calorimeter Instruction Manual 5-1 MENU DESCRIPTIONS Note: Keys which make global changes to the setup of the calorimeter contain a YES or NO r

6400 Calorimeter Instruction Manual 5-2 Start Preweigh: This key is used to start the sample pre-weigh process. The user is presented with or prom

6400 Calorimeter Instruction Manual 5-3 Bucket Min Value: Press this key to access its numeric dialog box to set a minimum bucket value. Jacket Plot

6400 Calorimeter Instruction Manual 5-4 Spiking Correction: Accesses the Spike Controls sub-menu: “Spiking” is the addition of material, such as ben

6400 Calorimeter Instruction Manual 5-5  Reset Rinse Tank Counter. Resets the counter when the rinse tank has been refilled. This counter must b

6400 Calorimeter Instruction Manual 5-6 Print Error Messages: When turned ON, all error messages will be printed on the printer as well as displayed

6400 Calorimeter Instruction Manual 5-7  User Setup ID Used to enter a unique identifier for recalling user settings. Parr offers a unique progra

6400 Calorimeter Instruction Manual 1-1 PREFACE Scope This manual contains instructions for installing and operating the Parr 6400 Calorimeter. Fo

6400 Calorimeter Instruction Manual 5-8 Calibration Data and Controls Menu Calibration Run Limit: Displays the maximum number of runs that will be

6400 Calorimeter Instruction Manual 5-9 Bomb 1: Leads to sub-menu, Bomb 1. Displays standardization information for bomb and bucket combinations.

6400 Calorimeter Instruction Manual 5-10 Print Standardization Runs: This key will print all of the tests that have been incorporated into the calcu

6400 Calorimeter Instruction Manual 5-11 Thermochemical Corrections Menu The Thermochemical Corrections Menu permits three types of fixed correctio

6400 Calorimeter Instruction Manual 5-12 Fixed Acid Correction: Press this key on the LEFT side to toggle ON or OFF the fixed acid correction for d

6400 Calorimeter Instruction Manual 5-13 Sulfur Value is Percent: When set to ON, the sulfur value is being entered as weight percent sulfur. If an

6400 Calorimeter Instruction Manual 5-14 Moisture Multiplier: Press to access the Moisture Multiplier numeric dialog box and set the value. This v

6400 Calorimeter Instruction Manual 5-15 Next Auto Sample ID Number: Establishes the initial sample number for a series of tests and then shows the

6400 Calorimeter Instruction Manual 5-16 Reporting Controls Menu Report Width: Toggle this key to set the column width of the printer to either 40 o

6400 Calorimeter Instruction Manual 5-17 Printer Port (RS232): Accesses sub-menu, Printer Port Communications. Sets the communication parameters fo

6400 Calorimeter Instruction Manual 1-2 Purpose Heats of combustion, as determined in an oxygen bomb calorimeter such as the 6400 Isoperibol Calorim

6400 Calorimeter Instruction Manual 5-18 • Parity. Standard options for parity. Choose from None, Odd or Even. • Number of Stop Bits. Standard op

6400 Calorimeter Instruction Manual 5-19 Further information on establishing communications for the Printer Port, Balance Port, Network Interface, B

6400 Calorimeter Instruction Manual 5-20 Select: This key is used to begin the file selection process. The up / down and page up / page down keys ar

6400 Calorimeter Instruction Manual 5-21 Data Logger: Displays ON/OFF status and accesses the Data Logger Controls Menu for setting the specific log

6400 Calorimeter Instruction Manual 5-22 View System Log: This key accesses its sub-menu which displays the contents of /flash/log/messages. This f

6400 Calorimeter Instruction Manual 5-23 I/O Diagnostics: Press this key to display the I/O Diagnostics sub-menu, which allows the user to manipula

6400 Calorimeter Instruction Manual 6-1 CALCULATIONS Corrections Fuse Correction There are two components to the fuse correction in the 6400 Calori

6400 Calorimeter Instruction Manual 6-2 This factor is added to the calculations when Spike Controls, Use Spiking is set to ON. The Heat of Combust

6400 Calorimeter Instruction Manual 6-3 Manual Entry During the reporting process, the controller will prompt the user to enter the following values

6400 Calorimeter Instruction Manual 6-4 Heat of formation of sulfuric acid (from SO2) is 36.1 calories / milliequivalent. Sample mass is the mass

6400 Calorimeter Instruction Manual 1-3 Safety Information To avoid electrical shock, always: 1. Use a properly grounded electrical outlet of corre

6400 Calorimeter Instruction Manual 6-5 Example 2: The following assumptions are made and outlined in D240. 1) The acid value is ALL nitric 2) Th

6400 Calorimeter Instruction Manual 6-6 ASTM, ISO and Other Methods Current ASTM, ISO, and British Standard Methods differ on their treatment of the

6400 Calorimeter Instruction Manual 6-7 The values for fixed acid and sulfur, which are used in preliminary reports, will reflect a sulfur correcti

6400 Calorimeter Instruction Manual 7-1 REPORTS The 6400 Calorimeter can transmit its stored test data in either of two ways. The Auto Report Dest

6400 Calorimeter Instruction Manual 7-2 The DESEL ALL key is used to cancel the current selection of files. To bring the selected report or series o

6400 Calorimeter Instruction Manual 8-1 MEMORY MANAGEMENT The 6400 Calorimeter will hold data for 1000 tests in its memory. These tests may be pre

6400 Calorimeter Instruction Manual 9-1 MAINTENANCE Note: Some of the following manual sections contain information in the form of warnings, cautio

6400 Calorimeter Instruction Manual 9-2 2. Use a non-metallic object, such as the rounded corner of a plastic credit card, to simply pry the seal

6400 Calorimeter Instruction Manual 9-3 50 to 100 Test Maintenance Replace the heating wire, with 2” of 840DD2. Wind the wire 360 degrees clockwise

6400 Calorimeter Instruction Manual 9-4 7. Remove the cylinder spacer, 1141DD, which sits on top of the snap ring, 1137DD. 8. Remove the snap ring

6400 Calorimeter Instruction Manual 2-1 INSTALLATION Note: Some of the following manual sections contain information in the form of warnings, cauti

6400 Calorimeter Instruction Manual 10-1 TROUBLESHOOTING Bomb Exhaust Troubleshooting The bomb exhaust and sealing is controlled by movement of the

6400 Calorimeter Instruction Manual 10-2 Confirm function of the 966DD2 piston In order to reduce the amount of time it takes to duplicate and troub

6400 Calorimeter Instruction Manual 10-3 Jacket Temperature Troubleshooting The jacket temperature is monitored with the use of a thermistor install

6400 Calorimeter Instruction Manual 10-4 A Preperiod Timeout Has Occurred The calorimeter has failed to establish an acceptable initial temperature,

6400 Calorimeter Instruction Manual 10-5 You Have Exceeded the Run Data File Limit (1000 Files) The memory set aside for test runs has been filled.

6400 Calorimeter Instruction Manual 11-1 TECHNICAL SERVICE Contact Us Should you need assistance in the operation or service of your instrument, pl

6400 Calorimeter Instruction Manual 12-1 PARTS LIST Principal Assemblies in Calorimeter Item Description 1138/1138CL 1795E 1796E 897E A1250DD A125

6400 Calorimeter Instruction Manual 12-2 A1457DD Accessory / Installation Kit Parts List Item Description 231C2 3415 356HCW 43AS 811DD 840DD2 845DD

6400 Calorimeter Instruction Manual 12-3 A1266DD Cover Assembly Parts List Item Description Contact Pin Assembly 986DD 987DD 988DD 989DD 1021DD SN1

6400 Calorimeter Instruction Manual 13-1 DRAWINGS Figure 10 - 1138 Parts Diagram

6400 Calorimeter Instruction Manual 2-2 tighten slightly with a wrench. Smaller tube sizes (up to 3/16” or 4mm) take less tightening to reach the o

6400 Calorimeter Instruction Manual 13-2 1138 Parts Diagram Key Key No. Item Description 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21

6400 Calorimeter Instruction Manual 13-3 Figure 11 - 6400 Cutaway Right

6400 Calorimeter Instruction Manual 13-4 Figure 12 - 6400 Cutaway Left

6400 Calorimeter Instruction Manual 13-5 Figure 13 - 6400 Cover Open

6400 Calorimeter Instruction Manual 13-6 Figure 14 - A1250DD Control Schematic

6400 Calorimeter Instruction Manual 13-7 Figure 15 - A1251DD Oxygen Solenoid Assembly Figure 16 – A1447DD Water Solenoid Assembly

6400 Calorimeter Instruction Manual 13-8 Figure 17 – A1435DD Rinse Valve Assembly

6400 Calorimeter Instruction Manual 13-9 Figure 18 - 6400 Internal Plumbing Diagram

6400 Calorimeter Instruction Manual 13-10 Figure 19 - 6400 Water Tank and Jacket Cooling Solenoid

6400 Calorimeter Instruction Manual 13-11 Figure 20 – A1455DD Propeller Assembly Apply thread sealant (Locktite or equivalent) to set screw in 12

6400 Calorimeter Instruction Manual 2-3 Figure 1 - 6400 Calorimeter Back Panel - Label Water Connection Remove the cap plug on the water filling

6400 Calorimeter Instruction Manual 13-12 Figure 22 - A1268DD Stirrer motor and Mount

6400 Calorimeter Instruction Manual 13-13 Figure 23 – 6400 Bucket Assembly

6400 Calorimeter Instruction Manual 13-14 Figure 24 - 6400 Air Can Assembly, Cutaway Left

6400 Calorimeter Instruction Manual 13-15 Figure 25 - Air Can Assembly, Cutaway Front

6400 Calorimeter Instruction Manual 13-16 Figure 26 - A1450DD Bomb Head Assembly, View 1

6400 Calorimeter Instruction Manual 13-17 Figure 27 - A1450DD Bomb Head Assembly, View 2

6400 Calorimeter Instruction Manual 13-18 Figure 28 – A1050DD Rinse Collection Assembly

6400 Calorimeter Instruction Manual 13-19 Figure 29 - Wiring Diagram

6400 Calorimeter Instruction Manual 13-20 Figure 30 - Wiring Diagram

6400 Calorimeter Instruction Manual 13-21 Figure 31 – Fuse Diagram